(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

Base Information

Chemical Name:(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol
CAS No.:1616111-60-4
Molecular Formula:C₁₈H₂₆O₁₁
Molecular Weight:418.398
Hs Code.:

(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

Synonyms:(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

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Chemical Property of (2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

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Technology Process of (2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

There total 7 articles about (2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: [(2R,3R,4R,5R,6R)-3,4,5-triacetoxy-6-[3-[(2R,3S,4S,5R,6R)-3,4,5-triacetoxy-6-(acetoxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-2-yl]methyl acetate

: 1616111-60-4
(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

Guidance literature:: With methanol; sodium methylate; at 20 ℃;

Reference yield:

: 1453855-86-1
(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-(3-hydroxyphenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1616111-60-4
(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 18 h / 0 - 40 °C

2: sodium methylate; methanol / 20 °C

With methanol; boron trifluoride diethyl etherate; sodium methylate; In dichloromethane;

Reference yield:

: 1453855-64-5
[(2R,3S,6S)-3-acetoxy-6-[3-[tert-butyl(dimethyl)silyl]oxyphenyl]-3,6-dihydro-2H-pyran-2-yl]methyl acetate

: 1616111-60-4
(2R,3S,4R,5S,6R)-2-(hydroxymethyl)-6-[3-[(2R,3S,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxyphenyl]tetrahydropyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 5 steps

1: 4-methylmorpholine N-oxide; 2,6-dimethylpyridine; methanesulfonamide; osmium(VIII) oxide / water; tert-butyl alcohol / 20 °C

2: 2,6-dimethylpyridine; dmap / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.5 h / 20 °C

4: boron trifluoride diethyl etherate / dichloromethane / 18 h / 0 - 40 °C

5: sodium methylate; methanol / 20 °C

With 2,6-dimethylpyridine; methanol; dmap; osmium(VIII) oxide; methanesulfonamide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium methylate; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;