C₁₇H₂₇NO₂

Base Information

• Chemical Name: C₁₇H₂₇NO₂
• CAS No.: 1404069-57-3
• Molecular Formula: C₁₇H₂₇NO₂
• Molecular Weight: 277.407
• Mol file: 1404069-57-3.mol

Synonyms:C₁₇H₂₇NO₂

Chemical Property of C₁₇H₂₇NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₇NO₂

There total 5 articles about C₁₇H₂₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C17H25N3O2 (1404069-64-2) → C17H27NO2 (1404069-57-3)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; water; at 70 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c2ob26649k

Reference yield:

(S)-1-(4-Methoxy-benzyloxy)-non-8-en-3-ol (474254-69-8) → C17H27NO2 (1404069-57-3)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 2.25 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 20 h / Inert atmosphere; Heating

3: triphenylphosphine / tetrahydrofuran; water / 3 h / 70 °C / Inert atmosphere

With sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide; 3: |Staudinger Azide Reduction;

DOI:10.1039/c2ob26649k

Reference yield:

C18H28O5S (1404069-73-3) → C17H27NO2 (1404069-57-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 20 h / Inert atmosphere; Heating

2: triphenylphosphine / tetrahydrofuran; water / 3 h / 70 °C / Inert atmosphere

With sodium azide; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2: |Staudinger Azide Reduction;

DOI:10.1039/c2ob26649k

upstream raw materials:

(S)-1-(4-Methoxy-benzyloxy)-non-8-en-3-ol

C₁₇H₂₅N₃O₂

C₁₈H₂₈O₅S

(R)-2-(2-((4-methoxybenzyl)oxy)ethyl)oxirane

Downstream raw materials:

C₂₇H₃₅NO₄

C₂₉H₃₇NO₅

C₂₇H₃₃NO₅

C₂₇H₃₃NO₅