lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

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Chemical Name:lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate
CAS No.:1622069-08-2
Molecular Formula:C₂₆H₂₀N₅O₃*Li
Molecular Weight:457.417
Hs Code.:

Synonyms:lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

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Chemical Property of lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

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Technology Process of lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

There total 5 articles about lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1622069-07-1
methyl 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

: 1622069-08-2
lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 20 ℃; for 12h;

Reference yield:

: 1622068-55-6
3-[3-(3-hydroxymethyl-phenyl)-6-oxo-6H-pyridazin-1-ylmethyl]-benzoic acid methyl ester

: 1622069-08-2
lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / dichloromethane / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 75 °C

3: lithium hydroxide monohydrate / water; tetrahydrofuran / 12 h / 20 °C

With lithium hydroxide monohydrate; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1622068-56-7
methyl 3-((3-(3-(bromomethyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

: 1622069-08-2
lithium 3-((3-(3-((2-amino-1H-benzo[d]imidazol-1-yl)methyl)phenyl)-6-oxopyridazin-1(6H)-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 75 °C

2: lithium hydroxide monohydrate / water; tetrahydrofuran / 12 h / 20 °C

With lithium hydroxide monohydrate; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;