(1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

Base Information

Chemical Name:(1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine
CAS No.:1232683-19-0
Molecular Formula:C₂₀H₂₇NO₂S
Molecular Weight:345.506
Hs Code.:

Synonyms:(1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

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Technology Process of (1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

There total 1 articles about (1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 862776-58-7
(S)-N-benzylidene-2-methylpropane-2-sulfinamide

: C₉H₁₀LiO^(1-)*Li⁽¹⁺⁾

: (1R,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

: 1232683-19-0
(1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

Guidance literature:: C₉H₁₀LiO^(1-)*Li⁽¹⁺⁾; With dimethyl zinc(II); In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

(S)-N-benzylidene-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at -65 ℃; for 12h; Inert atmosphere;

With water; In tetrahydrofuran; at -65 - 20 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/ejoc.201000111

Reference yield:

: 1232683-19-0
(1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

: 1232683-33-8
(S)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine

Guidance literature:: (1S,S(S))-N-(tert-butylsulfinyl)-2-[2-(2-hydroxyethyl)phenyl]-1-phenylethanamine; With hydrogenchloride; In 1,4-dioxane; methanol; at 0 ℃; for 3h;

With sodium hydrogencarbonate; In 1,4-dioxane; methanol; water;
DOI:10.1002/ejoc.201000111