2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol

Base Information

• Chemical Name: 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol
• CAS No.: 872398-92-0
• Molecular Formula: C₄₂H₅₄O₉S₄
• Molecular Weight: 831.149

Synonyms:2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol

Chemical Property of 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol

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Technology Process of 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol

There total 1 articles about 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Toluene-4-sulfonic acid 2-(2-{(E)-4'-[2-(2-hydroxy-ethoxy)-ethoxymethyl]-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy}-ethoxy)-ethyl ester + 5-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-ol (872398-90-8) → 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol (872398-92-0)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetonitrile; for 16h; Heating;

DOI:10.1055/s-2005-918468

Reference yield: 84.0%

2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol (872398-92-0) + p-toluenesulfonyl chloride (98-59-9) → C49H60O11S5 (957140-90-8)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 15h;

DOI:10.1021/ja0724590

Reference yield: 60.0%

2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-Diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethanol (872398-92-0) + (4,7-bis-bromomethyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetic acid (753006-59-6) → (4,7-Bis-bromomethyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetic acid 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethyl ester (872398-94-2)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

DOI:10.1055/s-2005-918468

upstream raw materials:

5-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-ol

Downstream raw materials:

(4,7-Bis-bromomethyl-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetic acid 2-[2-((E)-4'-{2-[2-(5-{2-[2-(2,6-diisopropyl-phenoxy)-ethoxy]-ethoxy}-naphthalen-1-yloxy)-ethoxy]-ethoxymethyl}-[2,2']bi[[1,3]dithiolylidene]-4-ylmethoxy)-ethoxy]-ethyl ester

C₄₉H₆₀O₁₁S₅

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