benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

Base Information

Chemical Name:benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate
CAS No.:1042432-14-3
Molecular Formula:C₃₁H₃₄N₂O₄S
Molecular Weight:530.688
Hs Code.:

Synonyms:benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

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Chemical Property of benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

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Technology Process of benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

There total 1 articles about benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 28092-52-6
(3aS,6aR)-1,3-dibenzyltetrahydro-1H-thieno[3,4-d]imidazole-2,4-dione

: 118058-70-1
benzyl 5-iodopentanoate

: 1042432-14-3
benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

Guidance literature:: benzyl 5-iodopentanoate; With bromine; zinc; In tetrahydrofuran; toluene; at 50 - 60 ℃; for 1h;

(3aS,6aR)-1,3-dibenzyltetrahydro-1H-thieno[3,4-d]imidazole-2,4-dione; nanopalladium catalyst; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; at 30 ℃; for 24h; Further stages.;
DOI:10.1016/j.tetasy.2008.05.020

Reference yield: 95.0%

: 1042432-14-3
benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate

: C₃₁H₃₂N₂O₃S

Guidance literature:: benzyl (3aS,6aR)-5-(1,3-dibenzyl-2,3,3a,4,6,6a-hexahydro-2-oxo-4-hydroxyl-1H-thieno[3,4-d]imidazol-4-yl)pentanoate; With hydrogenchloride; In water; toluene; at 60 ℃; for 5h;

With sodium hydrogencarbonate; In water; toluene;