Technology Process of butyl-2-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-methylbutanoate
There total 6 articles about butyl-2-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-methylbutanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol;
at 20 ℃;
for 18h;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / n-heptane; benzene; tetrahydrofuran / 1 h / -40 °C / Inert atmosphere
1.2: 2.25 h / -40 °C
2.1: camphor-10-sulfonic acid / toluene / Dean-Stark system; Reflux
3.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 20 °C / 760.05 Torr
With
hydrogen; lithium diisopropyl amide;
palladium 10% on activated carbon; camphor-10-sulfonic acid;
In
tetrahydrofuran; methanol; n-heptane; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / n-heptane; benzene; tetrahydrofuran / 1 h / -40 °C / Inert atmosphere
1.2: 2.25 h / -40 °C
2.1: camphor-10-sulfonic acid / toluene / Dean-Stark system; Reflux
3.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 20 °C / 760.05 Torr
With
hydrogen; lithium diisopropyl amide;
palladium 10% on activated carbon; camphor-10-sulfonic acid;
In
tetrahydrofuran; methanol; n-heptane; toluene; benzene;
