Technology Process of C29H34FNO7S
There total 4 articles about C29H34FNO7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H34FNO6S;
With
ozone;
In
dichloromethane;
at -78 ℃;
With
sodium tetrahydroborate;
In
dichloromethane;
at -78 - 25 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 8 h / -78 - 25 °C
2.1: ozone / dichloromethane / -78 °C
2.2: -78 - 25 °C
With
ozone; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydrogensulfite / ethanol; water / 0.5 h / 165 °C / microwave reactor
2.1: thionyl chloride / 3 h / Reflux
3.1: triethylamine / dichloromethane / 3 h / 0 - 25 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
5.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
5.2: 8 h / -78 - 25 °C
6.1: ozone / dichloromethane / -78 °C
6.2: -78 - 25 °C
With
thionyl chloride; ozone; sodium hydrogensulfite; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; dichloromethane; water;