Technology Process of C47H55NO12
There total 5 articles about C47H55NO12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
Inert atmosphere;
Reflux;
DOI:10.1002/chem.201200887
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; triethylamine / dichloromethane / 4 h / 20 °C
2: boron trifluoride diethyl etherate / -40 - -20 °C
3: hydrogen fluoride / water; acetonitrile / 20 °C
4: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Inert atmosphere; Reflux
With
dmap; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; hydrogen fluoride; tri-n-butyl-tin hydride; triethylamine;
In
dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/chem.201200887
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate / -40 - -20 °C
2: hydrogen fluoride / water; acetonitrile / 20 °C
3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Inert atmosphere; Reflux
With
2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; hydrogen fluoride; tri-n-butyl-tin hydride;
In
water; toluene; acetonitrile;
DOI:10.1002/chem.201200887