1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

Base Information

Chemical Name:1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol
CAS No.:355014-77-6
Molecular Formula:C₃₅H₃₉NO₅
Molecular Weight:553.698
Hs Code.:

Synonyms:1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

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Chemical Property of 1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

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Technology Process of 1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

There total 3 articles about 1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 355014-76-5
1,3,4,5-tetra-O-benzyl-7-O-(t-butyldimethylsilyl)-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

: 355014-77-6
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 55 ℃;
DOI:10.1016/S0968-0896(00)00343-6

Reference yield:

: 355014-75-4
3,4,5,7-tetra-O-benzyl-1-O-(t-butyldimethylsilyl)-L-arabino-2,6-heptodiulose

: 355014-77-6
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

Guidance literature:: Multi-step reaction with 2 steps

1: 577 mg / ammonium formate; molecular sieves 3A; NaBH₃CN / methanol / 1 h / 20 °C

2: 78 percent / acetic acid / tetrahydrofuran; H₂O / 55 °C

With 3 A molecular sieve; ammonium formate; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; water;
DOI:10.1016/S0968-0896(00)00343-6

Reference yield:

: 1,3,4,5-tetra-O-benzyl-7-O-(t-butyldimethylsilyl)-L-galacto-heptitol

: 355014-77-6
1,3,4,5-tetra-O-benzyl-2,6-dideoxy-2,6-imino-L-glycero-L-galacto-heptitol

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; dimethyl sulfoxide; triethylamine / CH₂Cl₂ / -78 - 20 °C

2: 577 mg / ammonium formate; molecular sieves 3A; NaBH₃CN / methanol / 1 h / 20 °C

3: 78 percent / acetic acid / tetrahydrofuran; H₂O / 55 °C

With oxalyl dichloride; 3 A molecular sieve; ammonium formate; sodium cyanoborohydride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1: Swern oxidation;
DOI:10.1016/S0968-0896(00)00343-6