(3,5-dimethylphenyl)trimethylstannane

Base Information

Chemical Name:(3,5-dimethylphenyl)trimethylstannane
CAS No.:260269-19-0
Molecular Formula:C₁₁H₁₈Sn
Molecular Weight:268.974
Hs Code.:

Synonyms:(3,5-dimethylphenyl)trimethylstannane

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Chemical Property of (3,5-dimethylphenyl)trimethylstannane

Chemical Property:

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Technology Process of (3,5-dimethylphenyl)trimethylstannane

There total 4 articles about (3,5-dimethylphenyl)trimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1-(3,5-dimethylphenyl)-2-(methylsulfonyl)diazene

: 661-69-8
hexamethyldistannane

: 260269-19-0
(3,5-dimethylphenyl)trimethylstannane

Guidance literature:: In acetonitrile; at 20 ℃; Irradiation; Inert atmosphere;
DOI:10.1021/acs.orglett.9b01788

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 260269-19-0
(3,5-dimethylphenyl)trimethylstannane

: 260269-20-3
[(CH₃)3Sn]2C₆H₃CH₃

: 937-01-9
trimethyl(3-methylphenyl)stannane

: 108-38-3,104809-90-7
m-xylene

: 108-67-8
1,3,5-trimethyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: further solvent(s)

2: CH₃Li / tetrahydrofuran; diethyl ether

With CH₃Li; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0022-328X(99)00471-4

Reference yield:

: 77-78-1
dimethyl sulfate

: 197141-36-9
1,3,5-tris(trimethylstannyl)benzene

: 260269-19-0
(3,5-dimethylphenyl)trimethylstannane

: 260269-20-3
[(CH₃)3Sn]2C₆H₃CH₃

: 937-01-9
trimethyl(3-methylphenyl)stannane

: 108-38-3,104809-90-7
m-xylene

: 108-67-8
1,3,5-trimethyl-benzene

Guidance literature:: With CH₃Li; In tetrahydrofuran; diethyl ether; (Ar); CH3Li in Et2O added dropwise to ((CH3)3Sn)3C6H3 in THF (-70°C); warmed to -50°C, stirred; (CH3)2SO4 added; further product;further intermediates; various yields of intermediates at various reactant ratios and addition orders; CH3OD added; warmed to room temp.; water and C6(CH3)6 added; extd. (Et2O); washed (water, brine); dried (MgSO4); identified by gas chromy.-massspectrometry; yields detd. by gas chromy.;
DOI:10.1016/S0022-328X(99)00471-4