1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

Base Information

Chemical Name:1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester
CAS No.:103047-58-1
Molecular Formula:C₂₄H₂₈O₃
Molecular Weight:364.485
Hs Code.:

Synonyms:1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

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Chemical Property of 1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

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Technology Process of 1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

There total 9 articles about 1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36440-65-0
8-methylnaphtho[1,2-c]furan-1,3-dione

: 103047-58-1
1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: LiAlH₄; THF

2: benzene; toluene; PBr₃

3: aqueous ethanol

4: aqueous H₂SO₄; acetic acid

5: polyphosphoric acid

6: amalgamated zinc; aqueous HCl

7: THF; LiAlH₄; diethyl ether

8: CCl₄; PBr₃

9: potassium

With tetrahydrofuran; hydrogenchloride; tetrachloromethane; lithium aluminium tetrahydride; PPA; amalgamated zinc; diethyl ether; ethanol; sulfuric acid; potassium; phosphorus tribromide; acetic acid; toluene; benzene;

Reference yield:

: 106736-50-9
1,2-bis-hydroxymethyl-7-methyl-naphthalene

: 103047-58-1
1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: benzene; toluene; PBr₃

2: aqueous ethanol

3: aqueous H₂SO₄; acetic acid

4: polyphosphoric acid

5: amalgamated zinc; aqueous HCl

6: THF; LiAlH₄; diethyl ether

7: CCl₄; PBr₃

8: potassium

With tetrahydrofuran; hydrogenchloride; tetrachloromethane; lithium aluminium tetrahydride; PPA; amalgamated zinc; diethyl ether; ethanol; sulfuric acid; potassium; phosphorus tribromide; acetic acid; toluene; benzene;

Reference yield:

: 100375-74-4
1,2-bis-bromomethyl-7-methyl-naphthalene

: 103047-58-1
1-[2-(8-methyl-acenaphthen-3-yl)-ethyl]-2-oxo-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: aqueous ethanol

2: aqueous H₂SO₄; acetic acid

3: polyphosphoric acid

4: amalgamated zinc; aqueous HCl

5: THF; LiAlH₄; diethyl ether

6: CCl₄; PBr₃

7: potassium

With tetrahydrofuran; hydrogenchloride; tetrachloromethane; lithium aluminium tetrahydride; PPA; amalgamated zinc; diethyl ether; ethanol; sulfuric acid; potassium; phosphorus tribromide; acetic acid;