exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione

Base Information

• Chemical Name: exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione
• CAS No.: 90036-80-9
• Molecular Formula: C₂₆H₂₄O₄S
• Molecular Weight: 432.54

Synonyms:exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione

Chemical Property of exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione

Chemical Property:

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Technology Process of exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione

There total 7 articles about exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C17H18O4 (36269-21-3) + 2-(phenylthio)-1,3-cyclopentanedione (90036-83-2) → exo-4-(1-phenylthiocyclopentyl-2,5-dione)hexacyclo<7.5.1.03.13.05.12.07.11.010.14>pentadecane-2,6-dione (90036-80-9)

Guidance literature:

With triethylamine; In benzene; for 40h; Heating;

Reference yield:

N-(phenylthio)succinimide (14204-24-1) → C26H24O4S (90036-80-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / triethylamine; benzene

2: 81 percent / Et₃N

With triethylamine; In triethylamine; benzene;

DOI:10.1016/S0040-4039(01)91138-4

Reference yield:

3-hydroxy-2-cyclopenten-1-one (5870-62-2) → C26H24O4S (90036-80-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / triethylamine; benzene

2: 81 percent / Et₃N

With triethylamine; In triethylamine; benzene;

DOI:10.1016/S0040-4039(01)91138-4

upstream raw materials:

N-(phenylthio)succinimide

C₂₀H₂₀O₄

3-hydroxy-2-cyclopenten-1-one

exo-4-(cyclopentyl-2,5-dione)-hexacyclo<7.5.1.0^3.13.0^5.12.0^7.11.0^10.14>pentadecane-2,6-dione

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