6-Methyl-alpha-phenyl-3-pyridazineethanethioamide

Base Information

Chemical Name:6-Methyl-alpha-phenyl-3-pyridazineethanethioamide
CAS No.:66978-42-5
Molecular Formula:C₁₃H₁₃N₃S
Molecular Weight:243.332
Hs Code.:
DSSTox Substance ID:DTXSID40985786
Nikkaji Number:J395.003D
Mol file:66978-42-5.mol

Synonyms:6-Methyl-alpha-phenyl-3-pyridazineethanethioamide;M 76011;66978-42-5;BRN 5534758;3-Pyridazineethanethioamide, 6-methyl-alpha-phenyl-;SCHEMBL11498796;DTXSID40985786;LS-129587;M-76010;2-(6-Methylpyridazin-3-yl)-2-phenylethanimidothioic acid

Suppliers and Price of 6-Methyl-alpha-phenyl-3-pyridazineethanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 6-Methyl-alpha-phenyl-3-pyridazineethanethioamide

Chemical Property:

Vapor Pressure:4E-09mmHg at 25°C
Boiling Point:473.2°C at 760 mmHg
Flash Point:240°C
PSA：88.43000
Density:1.232g/cm³
LogP:2.92370
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:243.08301860
Heavy Atom Count:17
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN=C(C=C1)C(C2=CC=CC=C2)C(=S)N

Technology Process of 6-Methyl-alpha-phenyl-3-pyridazineethanethioamide

There total 3 articles about 6-Methyl-alpha-phenyl-3-pyridazineethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-79-5
3-chloro-6-methylpyridazine

: 66978-42-5
2-(6-methyl-3-pyridazinyl)-2-phenylthioacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium amide / benzene / 1.) 6 h, room temperature, 2.) 4 h, reflux

2: 1.) triethylamine, 2.) hydrogen sulfide / 1.) pyridine, 30 min, room temperature, 2.) pyridine, 20 min, 0 deg C, 2 days, room temperature

With hydrogen sulfide; sodium amide; triethylamine; In benzene;
DOI:10.1248/cpb.29.3433

Reference yield:

: 140-29-4
phenylacetonitrile

: 66978-42-5
2-(6-methyl-3-pyridazinyl)-2-phenylthioacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / sodium amide / benzene / 1.) 6 h, room temperature, 2.) 4 h, reflux

2: 1.) triethylamine, 2.) hydrogen sulfide / 1.) pyridine, 30 min, room temperature, 2.) pyridine, 20 min, 0 deg C, 2 days, room temperature

With hydrogen sulfide; sodium amide; triethylamine; In benzene;
DOI:10.1248/cpb.29.3433

Reference yield:

: 73535-71-4
(6-Methyl-pyridazin-3-yl)-phenyl-acetonitrile

: 66978-42-5
2-(6-methyl-3-pyridazinyl)-2-phenylthioacetamide

Guidance literature:: With hydrogen sulfide; triethylamine; Yield given. Multistep reaction; 1.) pyridine, 30 min, room temperature, 2.) pyridine, 20 min, 0 deg C, 2 days, room temperature;
DOI:10.1248/cpb.29.3433