benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

Base Information

Chemical Name:benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside
CAS No.:86049-06-1
Molecular Formula:C₅₃H₅₄O₁₀
Molecular Weight:851.006
Hs Code.:

Synonyms:benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

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Chemical Property of benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

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Technology Process of benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

There total 3 articles about benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79936-13-3
benzyl exo-3,4-O-benzylidene-β-L-arabinopyranoside

: 86049-06-1
benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 31.9 percent / Hg(CN)2 / benzene; nitromethane / 20 h / 60 °C

2: 1) 1N NaOMe; 2) KOH / 1) MeOH, room temp., 16 h; 2) 100 deg C, 4 h

With potassium hydroxide; sodium methylate; mercury(II) cyanide; In nitromethane; benzene;
DOI:10.1016/0040-4020(82)85034-5

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 86049-06-1
benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 31.9 percent / Hg(CN)2 / benzene; nitromethane / 20 h / 60 °C

2: 1) 1N NaOMe; 2) KOH / 1) MeOH, room temp., 16 h; 2) 100 deg C, 4 h

With potassium hydroxide; sodium methylate; mercury(II) cyanide; In nitromethane; benzene;
DOI:10.1016/0040-4020(82)85034-5

Reference yield:

: 100-44-7
benzyl chloride

: 86049-04-9,86117-03-5
benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

: 86049-06-1
benzyl endo-3,4-O-benzylidene-2-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-L-arabinopyranoside

Guidance literature:: With potassium hydroxide; sodium methylate; Yield given. Multistep reaction; 1) MeOH, room temp., 16 h; 2) 100 deg C, 4 h;
DOI:10.1016/0040-4020(82)85034-5