5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

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Chemical Name:5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester
CAS No.:642442-34-0
Molecular Formula:C₅₉H₈₄O₂₃
Molecular Weight:1161.3
Hs Code.:

Synonyms:5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

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Chemical Property of 5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

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Technology Process of 5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

There total 1 articles about 5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 288850-04-4
3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide

: 642442-34-0
5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 48h; Heating;
DOI:10.1021/jo035040a

Reference yield: 89.0%

: 642442-34-0
5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

: 642442-37-3
{3-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenyl}-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 6h;
DOI:10.1021/jo035040a

Reference yield:

: 642442-34-0
5-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-isophthalic acid dimethyl ester

: Malonic acid mono-[3-[3,5-bis-(3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzyloxy)-benzyloxy]-5-(2-carboxy-acetoxymethyl)-benzyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / LiAlH₄ / tetrahydrofuran / 6 h / 0 °C

2: 100 percent / 4 h / 120 °C

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo035040a