4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

Base Information

Chemical Name:4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside
CAS No.:142329-93-9
Molecular Formula:C₂₆H₃₈N₂O₁₇
Molecular Weight:650.591
Hs Code.:

Synonyms:4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

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Chemical Property of 4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

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Technology Process of 4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

There total 7 articles about 4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 142329-92-8
4-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-3,4-O-isopropylidene-β-D-galactopyranoside

: 142329-93-9
4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

Guidance literature:: With water; trifluoroacetic acid; In chloroform; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield:

: 130572-04-2
methyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 142329-93-9
4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, r.t., 0.5 h, then cooled, 2.) r.t., 2 h

2: 1.) tetrabutylammonium bromide, CuBr₂, molecular sieves 4 Angstroem, 2.) 0.01 M sodium methoxide, methanol / 1.) 1,2-dichloroethane, DMF, r.t., 16 h, 2.) 2 h

3: 65 percent / trifluoroacetic acid, water / CHCl₃ / 2 h / Ambient temperature

With methanol; 4 A molecular sieve; tetrabutylammomium bromide; water; sodium methylate; sodium hydride; trifluoroacetic acid; copper(ll) bromide; In chloroform;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield:

: 130572-02-0
Methyl 3,4-O-Isopropylidene-2-O-(4-methoxybenzyl)-1-Thio-β-L-Fucopyranoside

: 142329-93-9
4-nitrophenyl O-α-L-fucopyranosyl-(1->3)-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrabutylammonium bromide, CuBr₂, molecular sieves 4 Angstroem, 2.) 0.01 M sodium methoxide, methanol / 1.) 1,2-dichloroethane, DMF, r.t., 16 h, 2.) 2 h

2: 65 percent / trifluoroacetic acid, water / CHCl₃ / 2 h / Ambient temperature

With methanol; 4 A molecular sieve; tetrabutylammomium bromide; water; sodium methylate; trifluoroacetic acid; copper(ll) bromide; In chloroform;
DOI:10.1016/S0008-6215(00)90562-7