6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

Base Information

Chemical Name:6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide
CAS No.:105537-61-9
Molecular Formula:Br*C₁₆H₂₀N₃O₂
Molecular Weight:366.258
Hs Code.:

Synonyms:6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

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Chemical Property of 6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

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Technology Process of 6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

There total 5 articles about 6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105537-95-9
6-Amino-1-(3-ethoxycarbonyl-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

: 105537-61-9
6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

Guidance literature:: With hydrogen bromide; In acetic acid; at 100 ℃; for 10h;
DOI:10.1021/jm00385a003

Reference yield:

: 28657-39-8
3-chloro-4-methyl-6-phenylpyridazine

: 105537-61-9
6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / butan-1-ol / 6 h / 100 °C

2: H₂ / Raney Ni / methanol / 20 °C / 760 Torr

3: dimethylformamide / 8 h / 80 °C

4: 48percentHBr / acetic acid / 10 h / 100 °C

With hydrogen bromide; hydrogen; hydrazine hydrate; nickel; In methanol; acetic acid; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jm00385a003

Reference yield:

: 13300-09-9
4-methyl-6-phenylpyridazin-3(2H)-one

: 105537-61-9
6-Amino-1-(3-carboxy-1-methyl-propyl)-5-methyl-3-phenyl-pyridazin-1-ium; bromide

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus oxychloride / 4 h / 85 - 95 °C

2: hydrazine hydrate / butan-1-ol / 6 h / 100 °C

3: H₂ / Raney Ni / methanol / 20 °C / 760 Torr

4: dimethylformamide / 8 h / 80 °C

5: 48percentHBr / acetic acid / 10 h / 100 °C

With hydrogen bromide; hydrogen; hydrazine hydrate; trichlorophosphate; nickel; In methanol; acetic acid; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jm00385a003