C₂₇H₃₇NO₈

Base Information

Chemical Name:C₂₇H₃₇NO₈
CAS No.:140181-48-2
Molecular Formula:C₂₇H₃₇NO₈
Molecular Weight:503.593
Hs Code.:

C<sub>27</sub>H<sub>37</sub>NO<sub>8</sub>

Synonyms:C₂₇H₃₇NO₈

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Chemical Property of C₂₇H₃₇NO₈

Chemical Property:

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Technology Process of C₂₇H₃₇NO₈

There total 14 articles about C₂₇H₃₇NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123218-01-9,130815-12-2
(1α,4aβ,8aβ)-(+/-)-1,2,3,4-tetrahydro-1-hydroxy-4,4,7,8a-tetramethyl-(4aH,8aH)-naphthalene-5,8-dione

: 140181-48-2
C₂₇H₃₇NO₈

Guidance literature:: Multi-step reaction with 11 steps

1: 80 percent / P₂O₅ / CHCl₃ / 2 h / 0 °C

2: 93 percent

3: 87 percent / H₂, quinoline / 10percent Pd/BaSO₄ / methanol / 2 h / 1551.4 Torr / Ambient temperature

4: 80 percent / sodium, methanol / 48 h / Heating

5: ozone, pyridine / CH₂Cl₂ / -78 °C

6: hydroxylamine hydrochloride, pyridine / ethanol / 0.75 h / Heating

7: DIBAH, pyridine / toluene / -78 °C

8: 96.7 percent / pyridine / 24 h / Ambient temperature

9: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 90 °C

10: 89 percent / zinc bromide / CH₂Cl₂ / 7 h / Ambient temperature

11: NaH / hexamethylphosphoric acid triamide; tetrahydrofuran

With pyridine; quinoline; methanol; hydroxylamine hydrochloride; hydrogen; sodium; phosphorus pentoxide; sodium hydride; diisobutylaluminium hydride; ozone; 3-chloro-benzenecarboperoxoic acid; zinc dibromide; Pd-BaSO₄; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; toluene;

Reference yield:

: 140181-33-5
(6aβ,9aβ,9bβ)-(+/-)-6a,7,8,9,9a,9b-hexahydro-4,7,7,9b-tetramethyl-(5H)-naphtho<1.8-de>-1,3-dioxin-6-one

: 140181-48-2
C₂₇H₃₇NO₈

Guidance literature:: Multi-step reaction with 12 steps

1: 1.) m-chloroperbenzoic acid 2.) silica gel / 1.) methylene dichloride, room temp., 3 h 2.) reflux, 15 h

2: 80 percent / P₂O₅ / CHCl₃ / 2 h / 0 °C

3: 93 percent

4: 87 percent / H₂, quinoline / 10percent Pd/BaSO₄ / methanol / 2 h / 1551.4 Torr / Ambient temperature

5: 80 percent / sodium, methanol / 48 h / Heating

6: ozone, pyridine / CH₂Cl₂ / -78 °C

7: hydroxylamine hydrochloride, pyridine / ethanol / 0.75 h / Heating

8: DIBAH, pyridine / toluene / -78 °C

9: 96.7 percent / pyridine / 24 h / Ambient temperature

10: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 90 °C

11: 89 percent / zinc bromide / CH₂Cl₂ / 7 h / Ambient temperature

12: NaH / hexamethylphosphoric acid triamide; tetrahydrofuran

With pyridine; quinoline; methanol; hydroxylamine hydrochloride; hydrogen; sodium; phosphorus pentoxide; silica gel; sodium hydride; diisobutylaluminium hydride; ozone; 3-chloro-benzenecarboperoxoic acid; zinc dibromide; Pd-BaSO₄; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; toluene;

Reference yield:

: 140181-32-4
(6α,6aβ,9aβ,9bβ)-(+/-)-6-hydroxy-5,6,6a,7,8,9,9a,9b-octahydro-4,7,7,9b-tetramethyl-naphtho<1.8-de>-1,3-dioxin

: 140181-48-2
C₂₇H₃₇NO₈

Guidance literature:: Multi-step reaction with 13 steps

1: 82 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 1.) m-chloroperbenzoic acid 2.) silica gel / 1.) methylene dichloride, room temp., 3 h 2.) reflux, 15 h

3: 80 percent / P₂O₅ / CHCl₃ / 2 h / 0 °C

4: 93 percent

5: 87 percent / H₂, quinoline / 10percent Pd/BaSO₄ / methanol / 2 h / 1551.4 Torr / Ambient temperature

6: 80 percent / sodium, methanol / 48 h / Heating

7: ozone, pyridine / CH₂Cl₂ / -78 °C

8: hydroxylamine hydrochloride, pyridine / ethanol / 0.75 h / Heating

9: DIBAH, pyridine / toluene / -78 °C

10: 96.7 percent / pyridine / 24 h / Ambient temperature

11: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 90 °C

12: 89 percent / zinc bromide / CH₂Cl₂ / 7 h / Ambient temperature

13: NaH / hexamethylphosphoric acid triamide; tetrahydrofuran

With pyridine; quinoline; methanol; hydroxylamine hydrochloride; hydrogen; sodium acetate; sodium; phosphorus pentoxide; silica gel; sodium hydride; diisobutylaluminium hydride; ozone; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; zinc dibromide; Pd-BaSO₄; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; toluene;