RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆

Base Information

• Chemical Name: RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆
• CAS No.: 104033-43-4
• Molecular Formula: C₄₈H₅₁NOP₃Ru*F₆P
• Molecular Weight: 996.894

Synonyms:RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆

Chemical Property of RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆

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Technology Process of RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆

There total 1 articles about RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCH₃(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

sodium hexaflorophosphate + RuCH3(CO)2(C41H39P3)(1+)*I(1-)=[RuCH3(CO)2(C41H39P3)]I (99299-59-9) + (+/-)sec-butyl isocyanide (14069-89-7) → RuCH3(CO)(C2H5CH(CH3)NC)(C41H39P3)(1+)*PF6(1-)=[RuCH3(CO)(C2H5CH(CH3)NC)(C41H39P3)]PF6 (104033-43-4)

Guidance literature:

With (CH₃)3NO; In ethanol; dichloromethane; N2-atmosphere; addn. of Me3NO to Ru-complex and the isonitrile in CH2Cl2; addn. of heptane after a few min; the obtained oil was dissolved in EtOH; addn. of an ethanolic soln. of NaPF6 to the filtered soln.;; cooling at -78°C for several h; the ppt. was filtered off, washed with ethanol, and dried; further pptn. by addn. of NaPF6 to the filtrate; elem. anal.;

DOI:10.1021/om00138a014

Reference yield: 70.0%

RuCH3(CO)(C2H5CH(CH3)NC)(C41H39P3)(1+)*PF6(1-)=[RuCH3(CO)(C2H5CH(CH3)NC)(C41H39P3)]PF6 (104033-43-4) → RuCl(CO)(C2H5CH(CH3)NC)(C41H39P3)(1+)*PF6(1-)=[RuCl(CO)(C2H5CH(CH3)NC)(C41H39P3)]PF6 (102261-56-3)

Guidance literature:

With HgCl₂; In dichloromethane; N2-atmosphere; addn. of HgCl2 to a CH2Cl2 soln. of the complex; reaction time: 7 min;; addn. of ethanol; partial evapn. under reduced pressure; ppt. was collected, washed with ethanol and pentane, and dried; elem. anal.;

DOI:10.1021/om00138a014

upstream raw materials:

RuCH₃(CO)2(C₄₁H₃₉P₃)⁽¹⁺⁾*I^(1-)=[RuCH₃(CO)2(C₄₁H₃₉P₃)]I

(+/-)sec-butyl isocyanide

Downstream raw materials:

RuCl(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)⁽¹⁺⁾*PF₆^(1-)=[RuCl(CO)(C₂H₅CH(CH₃)NC)(C₄₁H₃₉P₃)]PF₆

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