Technology Process of C58H81N10O13(3-)*Y(3+)
There total 8 articles about C58H81N10O13(3-)*Y(3+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
aq. acetate buffer;
at 90 ℃;
for 0.333333h;
pH=5;
- Guidance literature:
-
In
aq. acetate buffer;
at 90 ℃;
for 0.333333h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 1 h / 0 °C
2.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h
2.2: 18 h
3.1: water; lithium hydroxide / 1,4-dioxane / 5 h
3.2: pH 5 - 6
4.1: HATU; N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 0.08 h
4.2: 25 h / 20 - 65 °C
5.1: triisobutylsilane / dichloromethane / 5 h / 20 °C
6.1: aq. acetate buffer / 0.33 h / 90 °C
With
triisobutylsilane; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;
