11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

Base Information

Chemical Name:11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine
CAS No.:1252908-90-9
Molecular Formula:C₂₂H₂₁NO₂
Molecular Weight:331.414
Hs Code.:

Synonyms:11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

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Chemical Property of 11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

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Technology Process of 11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

There total 3 articles about 11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1252908-87-4
(E)-3-(2-morpholinobenzylidene)-5-phenylpent-4-yn-2-one

: 1252908-90-9
11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

Guidance literature:: With IPrAuOTf; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1039/c0cc01946a

Reference yield: 90.0%

: C₂₃H₂₃NO₂

: 1252908-90-9
11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)-1H-imidazol-2-(3H)-ylidene]gold(I)chloride; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 25 ℃; for 3h;
DOI:10.1002/chem.201201727

Reference yield: 8.0%

: 1252908-87-4
(E)-3-(2-morpholinobenzylidene)-5-phenylpent-4-yn-2-one

: 1252908-90-9
11-methyl-13-phenyl-3,4,10,13b-tetrahydro-1H-benzo[f]furo[3,4-c][1,4]oxazino[4,3-a]azepine

: 1-((4aSR,5RS)-5-(phenylethynyl)-1,2,4,4a,5,6-hexahydro-[1,4]oxazino[4,3-a]quinolin-5-yl)ethanone

Guidance literature:: With yttrium(III) trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 31h; diastereoselective reaction; Reflux; Molecular sieve;
DOI:10.1039/c0cc01946a