(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

Base Information

Chemical Name:(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside
CAS No.:134262-90-1
Molecular Formula:C₃₆H₄₀INO₁₁
Molecular Weight:789.618
Hs Code.:

(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

Synonyms:(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

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Chemical Property of (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

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Technology Process of (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

There total 11 articles about (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 134262-63-8
1,5-anhydro-2,4-dideoxy-3-O-methyl-4-phthalimido-L-threo-pent-1-enopyranose

: 134262-79-6
(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

: 134262-90-1
(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

: 2-{(3S,4R,5R)-6-[(2R,3S,4R,5R,6R)-5-Hydroxy-4,6-bis-(4-methoxy-benzyloxy)-2-methyl-tetrahydro-pyran-3-yloxy]-5-iodo-4-methoxy-tetrahydro-pyran-3-yl}-isoindole-1,3-dione

Guidance literature:: With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; In dichloromethane; at -23 - 25 ℃; for 6h;
DOI:10.1021/ja00126a013

Reference yield:

: 134262-62-7,134262-85-4
phenyl 2,4-dideoxy-3-O-methyl-4-phthalimido-1-thio-L-threo-pentopyranoside

: 134262-90-1
(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) m-CPBA / 1.) CH₂Cl₂, 2.) PhH, reflux

2: I⁽¹⁺⁾*ClO₄^(1-)-(sym-collidine)2 / CH₂Cl₂

With iodonium(di-γ-collidine) perchlorate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo951560x