C₆₁H₆₄O₁₀

Base Information

• Chemical Name: C₆₁H₆₄O₁₀
• CAS No.: 107855-16-3
• Molecular Formula: C₆₁H₆₄O₁₀
• Molecular Weight: 957.173
• Mol file: 107855-16-3.mol

Synonyms:C₆₁H₆₄O₁₀

Chemical Property of C₆₁H₆₄O₁₀

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₆₁H₆₄O₁₀

There total 2 articles about C₆₁H₆₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

benzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside (67831-42-9) + (2S,3R,4R,5S,6R)-3,4,5-Tris-benzyloxy-2-methyl-6-methylsulfanyl-tetrahydro-pyran (107802-80-2) → C61H64O10 (107855-16-3) + C61H64O10 (107855-17-4)

Guidance literature:

With 4 A molecular sieve; tetrabutylammomium bromide; silver trifluoromethanesulfonate; copper(ll) bromide; In nitromethane; at 20 ℃; for 4h; Bu₄NBr instead of AgOTf, ClCH₂CH₂Cl, DMF, 48 h;

DOI:10.1016/S0008-6215(00)90163-0

Reference yield:

benzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside (67831-42-9) + C37H46N3O4PS (130738-59-9) → C61H64O10 (107855-16-3) + C61H64O10 (107855-17-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; 2,6-lutidinium p-toluenesulfonate; 4 A molecular sieve; In dichloromethane; toluene; at 23 ℃; for 55h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)97729-3

upstream raw materials:

benzyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

(2S,3R,4R,5S,6R)-3,4,5-Tris-benzyloxy-2-methyl-6-methylsulfanyl-tetrahydro-pyran

C₃₇H₄₆N₃O₄PS