N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

Base Information

Chemical Name:N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide
CAS No.:1608159-79-0
Molecular Formula:C₁₇H₂₁N₃OSi
Molecular Weight:311.459
Hs Code.:

Synonyms:N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

Suppliers and Price of N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

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Technology Process of N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

There total 1 articles about N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1608160-06-0
N-(4-iodo-1-methyl-3-phenyl-1H-pyrazol-5-yl)acetamide

: 1066-54-2
trimethylsilylacetylene

: 1608159-79-0
N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

Guidance literature:: N-(4-iodo-1-methyl-3-phenyl-1H-pyrazol-5-yl)acetamide; With triethylamine; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;

trimethylsilylacetylene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Inert atmosphere; Sealed tube;

Reference yield:

: 1608159-79-0
N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

: 1608159-80-3
1-(5-amino-1-methyl-3-phenyl-pyrazol-4-yl)ethanone

Guidance literature:: With water; sodium hydroxide; In ethanol; at 90 ℃; for 6h;

Reference yield:

: 1608159-79-0
N-(1-methyl-3-phenyl-4-((trimethylsilyl)ethynyl)-1H-pyrazol-5-yl)acetamide

: 1608159-81-4
1-methyl-3-phenyl-pyrazolo[3,4-c]pyridazin-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol / 6 h / 90 °C

2: hydrogenchloride; sodium nitrite / dichloromethane; water / 1 h / -5 - 65 °C

With hydrogenchloride; water; sodium hydroxide; sodium nitrite; In ethanol; dichloromethane; water;