-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

Base Information

Chemical Name:-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester
CAS No.:78166-92-4
Molecular Formula:C₁₇H₂₁Cl₃N₂O₆
Molecular Weight:455.723
Hs Code.:

<N-<(Benzyloxy)carbonyl>-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

Synonyms:-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

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Chemical Property of -D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

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Technology Process of -D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

There total 2 articles about -D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 82377-03-5
N-<(Benzyloxy)carbonyl>-D-serine 2,4-Dinitrophenyl Ester

: 78166-90-2
N-Methyl-L-alanine 2,2,2-Trichloroethyl Ester

: 78166-92-4
-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

Guidance literature:: triethylamine; In dichloromethane; for 60h; Ambient temperature;
DOI:10.1021/jo00330a010

Reference yield:

: 78166-91-3
N-Methyl-L-alanine 2,2,2-Trichloroethyl Ester Hydrobromide

: 78166-92-4
-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 0.08 h / 0 °C

2: 88 percent / Et₃N / CH₂Cl₂ / 60 h / Ambient temperature

With triethylamine; triethylamine; In dichloromethane;
DOI:10.1021/jo00330a010

Reference yield: 87.5%

: 13734-41-3
t-Boc-L-valine

: 78166-92-4
-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

: 78166-93-5
-O<<(tert-butyloxy)carbonyl>-L-valyl>-D-seryl>-N-methyl-L-alanine 2,2,2-Trichloroethyl Ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In dichloromethane; 1.) 0 deg C, 3 h, 2.) room temperature, overnight;
DOI:10.1021/jo00330a010