N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

Base Information

Chemical Name:N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine
CAS No.:1415098-68-8
Molecular Formula:C₂₀H₂₇NO₄
Molecular Weight:345.439
Hs Code.:

Synonyms:N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

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Chemical Property of N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

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Technology Process of N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

There total 3 articles about N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1415098-65-5
N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

: 501-53-1,94274-21-2
benzyl chloroformate

: 1415098-68-8
N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c2ob26732b

Reference yield:

: (S,E)-N-((2,2-dimethyl-1,3-dioxolan-4-yl)methylene)but-3-en-1-amine

: 1415098-68-8
N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 0.17 h / -20 °C / Inert atmosphere

1.2: -20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1039/c2ob26732b

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 1415098-68-8
N-benzyloxycarbonyl-N-{(S)-1-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]allyl}-3-buten-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium sulfate / diethyl ether / 2 h / 20 °C

2.1: boron trifluoride diethyl etherate / diethyl ether / 0.17 h / -20 °C / Inert atmosphere

2.2: -20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With boron trifluoride diethyl etherate; magnesium sulfate; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1039/c2ob26732b