(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

Base Information

Chemical Name:(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2
CAS No.:108151-13-9
Molecular Formula:C₃₄H₂₄Co₂F₆O₄P₂
Molecular Weight:790.486
Hs Code.:

(CF<sub>3</sub>C<sub>2</sub>CF<sub>3</sub>)Co<sub>2</sub>(CO)4(((C<sub>6</sub>H<sub>5</sub>)2P)CH<sub>2</sub>)2

Synonyms:(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

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Chemical Property of (CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

Chemical Property:

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Technology Process of (CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

There total 4 articles about (CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 37685-63-5
{(carbonyl)3cobalt(μ-hexafluorobut-2-yne)cobalt(carbonyl)3}

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 108151-14-0
(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

: 108151-12-8
((CF₃C₂CF₃)Co₂(CO)5)2(((C₆H₅)2P)CH₂)2

: 108151-13-9
(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

Guidance literature:: With catalyst: benzophenone ketyl; In tetrahydrofuran; byproducts: CO; (Ar); at 293 K; ligand (0.061 mmol) and benzophenone ketyl (> 0.1 mL) added together via sep. necks to soln. of Co complex (0.058 mmol); immetiale color change (to deep red) observed; TLC analysis indicated completereact.; react. mechanism discussed; solvent removed in vac.; chromy. on silica gel plates (hexane/ether 20/1); 3 bands developed; each band eluated (CH2Cl2), recrystn. (hexane); band 1, 2, and 3 = Co4P2 compd. (elem. anal.), PCo-CoP compd. (oil), and Co-CoP2 compd. (elem. anal.), resp.;

Reference yield: 78.0%

: 37685-63-5
{(carbonyl)3cobalt(μ-hexafluorobut-2-yne)cobalt(carbonyl)3}

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 108151-12-8
((CF₃C₂CF₃)Co₂(CO)5)2(((C₆H₅)2P)CH₂)2

: 108151-13-9
(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

Guidance literature:: In hexane; (Ar); soln. of Co comlpex (0.065 mmol) and ligand (0.07 mmol) refluxed for 5 h; react. mechanism discussed; solvent removed in vac.; sepn. on silica gel (hexane/ether/CH2Cl2 10/1/1);

Reference yield:

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 108151-13-9
(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)CH₂)2

Guidance literature:: Multi-step reaction with 2 steps

1: catalyst: benzophenone ketyl / tetrahydrofuran

2: hexane

With catalyst: benzophenone ketyl; In tetrahydrofuran; hexane;