(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

Base Information

Chemical Name:(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid
CAS No.:161284-93-1
Molecular Formula:C₂₁H₂₀N₂O₅S
Molecular Weight:412.466
Hs Code.:

Synonyms:(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

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Chemical Property of (R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

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Technology Process of (R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

There total 4 articles about (R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 108-24-7
acetic anhydride

: 140645-73-4
(R)-3-(4-aminophenyl)-2-<(naphth-2-ylsulfonyl)amino>propionic acid

: 161284-93-1
(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1021/jm00049a008

Reference yield:

: 56613-61-7
(R)-4-nitro-phenylalanine

: 161284-93-1
(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1 N aq. NaOH / diethyl ether / 6 h / Ambient temperature

2: 59 percent / H₂ / Raney nickel / dimethylformamide / 48 h / 760 Torr

3: 39 percent / pyridine / Ambient temperature

With pyridine; sodium hydroxide; hydrogen; nickel; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm00049a008

Reference yield:

: 93-11-8
2-Naphthalenesulfonyl chloride

: 161284-93-1
(R)-3-<4-(acetylamino)phenyl>-2-<(naphth-2-ylsulfonyl)amino>propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1 N aq. NaOH / diethyl ether / 6 h / Ambient temperature

2: 59 percent / H₂ / Raney nickel / dimethylformamide / 48 h / 760 Torr

3: 39 percent / pyridine / Ambient temperature

With pyridine; sodium hydroxide; hydrogen; nickel; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jm00049a008