(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

Base Information

Chemical Name:(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine
CAS No.:198008-74-1
Molecular Formula:C₃₀H₃₂N₂
Molecular Weight:420.597
Hs Code.:

Synonyms:(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

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Chemical Property of (4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

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Technology Process of (4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

There total 3 articles about (4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 118628-68-5
(1R,2R)-(+)-N,N'-dimethyl-1,2-diphenyl-ethylenediamine

: 197898-62-7
(+/-)-3-(1-naphthyl)butanal

: 198008-74-1
(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

: 197898-63-8
(4R,5R)-1,3-Dimethyl-2-((R)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

Guidance literature:: In diethyl ether; at 20 ℃; for 15h;
DOI:10.1021/ja9708777

Reference yield:

: 172420-14-3
3-Naphthalen-1-yl-butyric acid methyl ester

: 198008-74-1
(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / LiAlH₄ / diethyl ether / 1.) 0 deg C, 5 min, 2.) 20 deg C, 30 min

2: 97 percent / DMSO, (COCl)2, Et₃N / CH₂Cl₂ / -60 - 20 °C

3: 86 percent / diethyl ether / 15 h / 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ja9708777

Reference yield:

: 78396-19-7
3-methyl-3-β-naphthylpropanol

: 198008-74-1
(4R,5R)-1,3-Dimethyl-2-((S)-2-naphthalen-1-yl-propyl)-4,5-diphenyl-imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / DMSO, (COCl)2, Et₃N / CH₂Cl₂ / -60 - 20 °C

2: 86 percent / diethyl ether / 15 h / 20 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ja9708777