C₄₃H₄₃N₅O₁₁

Base Information

Chemical Name:C₄₃H₄₃N₅O₁₁
CAS No.:923924-29-2
Molecular Formula:C₄₃H₄₃N₅O₁₁
Molecular Weight:805.841
Hs Code.:

C<sub>43</sub>H<sub>43</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:C₄₃H₄₃N₅O₁₁

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Chemical Property of C₄₃H₄₃N₅O₁₁

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Technology Process of C₄₃H₄₃N₅O₁₁

There total 8 articles about C₄₃H₄₃N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 923924-30-5
2-methoxy-5-methyl-3-nitro-benzoyl chloride

: 923924-34-9
C₃₄H₃₆N₄O₇

: 923924-29-2
C₄₃H₄₃N₅O₁₁

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 10h;
DOI:10.1021/jo0619940

Reference yield:

: 858848-07-4
2-methoxy-5-methyl-3-nitrobenzoic acid

: 923924-29-2
C₄₃H₄₃N₅O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl chloride; DMF / CDCl₃ / 6 h / 20 °C

2: 83 percent / triethylamine / CHCl₃ / 5 h / 20 °C

3: hydrogen / palladium on carbon / tetrahydrofuran / 8 h / 20 °C / 760 Torr

4: 61 percent / triethylamine / CHCl₃ / 5 h / 20 °C

5: hydrogen / palladium on carbon / tetrahydrofuran / 8 h / 20 °C / 760 Torr

6: 69 percent / triethylamine / CHCl₃ / 10 h / 20 °C

With oxalyl dichloride; hydrogen; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; chloroform-d1; chloroform;
DOI:10.1021/jo0619940

Reference yield:

: 923924-30-5
2-methoxy-5-methyl-3-nitro-benzoyl chloride

: 923924-29-2
C₄₃H₄₃N₅O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / triethylamine / CHCl₃ / 5 h / 20 °C

2: hydrogen / palladium on carbon / tetrahydrofuran / 8 h / 20 °C / 760 Torr

3: 61 percent / triethylamine / CHCl₃ / 5 h / 20 °C

4: hydrogen / palladium on carbon / tetrahydrofuran / 8 h / 20 °C / 760 Torr

5: 69 percent / triethylamine / CHCl₃ / 10 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; chloroform;
DOI:10.1021/jo0619940