3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

Base Information

Chemical Name:3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole
CAS No.:1179326-77-2
Molecular Formula:C₄₂H₃₂N₂O₁₁
Molecular Weight:740.723
Hs Code.:

Synonyms:3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

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Chemical Property of 3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

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Technology Process of 3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

There total 1 articles about 3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 286369-05-9
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl cyanide

: 207297-08-3
N-hydroxy-4-hydroxy-benzenecarboximidoyl chloride

: 1179326-77-2
3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

Guidance literature:: 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl cyanide; N-hydroxy-4-hydroxy-benzenecarboximidoyl chloride; In toluene; at 110 ℃; Inert atmosphere;

With triethylamine; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2009.04.036

Reference yield: 37.0%

: 1179326-77-2
3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole

: 1179326-84-1
5-(β-D-glucopyranosyl)-3-(4-hydroxyphenyl)-1,2,4-oxadiazole

Guidance literature:: 3-(4-hydroxyphenyl)-5-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-oxadiazole; With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 24h;

With Amberlite IR-120 resin; In methanol; dichloromethane; pH=5 - 6;
DOI:10.1016/j.bmc.2009.04.036