benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

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Chemical Name:benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside
CAS No.:132064-98-3
Molecular Formula:C₁₇H₁₈F₆N₂O₄
Molecular Weight:428.331
Hs Code.:

Synonyms:benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

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Chemical Property of benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

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Technology Process of benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

There total 6 articles about benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.36%

: 132064-96-1
benzyl 3,4-diamino-2,3,4,6-tetradeoxy-α-L-lyxo-hexopyranoside

: 407-25-0
trifluoroacetic anhydride

: 132064-98-3
benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

Guidance literature:: With triethylamine; In dichloromethane; at 4 ℃; for 16h;
DOI:10.1016/0008-6215(90)80086-I

Reference yield:

: 114413-02-4
benzyl 3-azido-2,3,6-trideoxy-α-L-arabino-hexopyranoside

: 132064-98-3
benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: ammonia / CHCl₃ / 1) r.t., 2 h, 2) 60 deg C, 9 h

3: hydrogen, triethylamine / 10percent Pd-C / ethanol / 8 h / 760 Torr / Ambient temperature

4: 68.36 percent / triethylamine / CH₂Cl₂ / 16 h / 4 °C

With pyridine; ammonia; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform;
DOI:10.1016/0008-6215(90)80086-I

Reference yield:

: 132064-97-2
benzyl 4-amino-3-azido-2,3,4,6-tetradeoxy-α-L-lyxo-hexopyranoside

: 132064-98-3
benzyl 2,3,4,6-tetradeoxy-3,4-bis(trifluoroacetamido)-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen, triethylamine / 10percent Pd-C / ethanol / 8 h / 760 Torr / Ambient temperature

2: 68.36 percent / triethylamine / CH₂Cl₂ / 16 h / 4 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/0008-6215(90)80086-I