isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

Base Information

Chemical Name:isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate
CAS No.:161403-79-8
Molecular Formula:C₂₀H₂₆O₄
Molecular Weight:330.424
Hs Code.:

Synonyms:isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

Suppliers and Price of isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

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Technology Process of isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

There total 2 articles about isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.6%

: 65-85-0,8013-63-6
benzoic acid

: 161403-78-7
isopropyl (1S,2S,3S,5S)-3-hydroxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

: 161403-79-8
isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 0.166667h;
DOI:10.3987/COM-94-S31

Reference yield:

: 117181-66-5
(1R,2S,3S,5S)-3-Hydroxy-5-isopropenyl-2-methyl-cyclopentanecarboxylic acid

: 161403-79-8
isopropyl (1S,2S,3R,5S)-3-benzoyloxy-5-isopropenyl-2-methylcyclopentane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 78.8 percent / K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

2: 98.6 percent / Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 0.17 h / 0 °C

With potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3987/COM-94-S31