1-thymine

Base Information

Chemical Name:1-thymine
CAS No.:220845-69-2
Molecular Formula:C₂₄H₂₆N₂O₄
Molecular Weight:406.481
Hs Code.:

1-<cis-2',cis-3'-bis(benzyloxymethyl)cyclopropyl>thymine

Synonyms:1-thymine

Suppliers and Price of 1-thymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-thymine

Chemical Property:

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Technology Process of 1-thymine

There total 6 articles about 1-thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: -3-(3''-methoxy-2''-methacryloyl)urea

: 220845-69-2
1-thymine

Guidance literature:: With ammonia; water; In methanol; at 85 ℃; for 24h;
DOI:10.1016/S0040-4020(98)01120-X

Reference yield:

: 172688-27-6
(1S,2R,3S)-2,3-Bis-benzyloxymethyl-cyclopropanecarbaldehyde

: 220845-69-2
1-thymine

Guidance literature:: Multi-step reaction with 6 steps

1: 71 percent / Jones' reagent / acetone / 10 h / -5 °C

2: 1.) ClCO₂Et, Et₃N, 2.) NH₃ / 1.) THF, -5 deg C, 1 h, 2.) THF, 0 deg C, 1 h

3: 78 percent / KOH, PhI(OAc)2 / 1 h / 5 - 20 °C

4: 83 percent / KOH / methanol / 48 h / Heating

5: 90 percent / benzene / 0.5 h / Heating

6: 57 percent / NH₃, H₂O / methanol / 24 h / 85 °C

With potassium hydroxide; jones' reagent; [bis(acetoxy)iodo]benzene; ammonia; water; chloroformic acid ethyl ester; triethylamine; In methanol; acetone; benzene;
DOI:10.1016/S0040-4020(98)01120-X

Reference yield:

: 220845-67-0
cis-2,cis-3-bis(benzyloxymethyl)cyclopropylamine

: 220845-69-2
1-thymine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / benzene / 0.5 h / Heating

2: 57 percent / NH₃, H₂O / methanol / 24 h / 85 °C

With ammonia; water; In methanol; benzene;
DOI:10.1016/S0040-4020(98)01120-X