tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate

Base Information

Chemical Name:tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate
CAS No.:1181693-05-9
Molecular Formula:C₂₅H₄₀O₅Si
Molecular Weight:448.675
Hs Code.:

Synonyms:tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate

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Technology Process of tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate

There total 1 articles about tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1181693-02-6
tert-butyl methyl 2-methylphenylmalonate

: 491879-65-3
methanesulfonic acid 2-(tert-butyl-dimethyl-silanyloxymethyl)allyl ester

: 1181693-05-9
tert-butyl methyl (2-(tert-butyldimethylsiloxy)methyl-2-propen-1-yl)(2-methylphenyl)malonate

Guidance literature:: tert-butyl methyl 2-methylphenylmalonate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h; Inert atmosphere;

methanesulfonic acid 2-(tert-butyl-dimethyl-silanyloxymethyl)allyl ester; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 55 ℃; for 86h; Inert atmosphere;
DOI:10.1021/ol901348f