2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

Base Information

Chemical Name:2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose
CAS No.:247214-70-6
Molecular Formula:C₂₉H₄₆O₆
Molecular Weight:490.681
Hs Code.:

Synonyms:2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

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Chemical Property of 2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

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Technology Process of 2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

There total 7 articles about 2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 247214-70-6
2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 1 h / 20 °C

2: mCPBA / CH₂Cl₂

3: AcOH / CH₂Cl₂ / 24 h

With acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; 1: Grignard reaction / 2: Epoxidation / 3: Cyclization;

Reference yield:

: 144489-81-6
3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-(tridec-2'-ynyl)-β-L-idofuranose

: 247214-70-6
2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / H₂, quinoline / 10 percent Pd/BaSO₄ / methanol / 760 Torr

2: mCPBA / CH₂Cl₂

3: AcOH / CH₂Cl₂ / 24 h

With quinoline; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; Pd-BaSO₄; In methanol; dichloromethane; 1: Reduction / 2: Epoxidation / 3: Cyclization;

Reference yield:

: C₁₄H₂₅BrMg

: 247214-70-6
2',5-anhydro-3-O-benzyl-6-deoxy-1,2-O-isopropylidene-6-C-[(2'S,3'S/2'R,3'R) and (2'S,3'R/2'R,3'S)-dihydroxytridecyl]-β-L-idofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 1 h / 20 °C

2: 74 percent / H₂, quinoline / 10 percent Pd/BaSO₄ / methanol / 760 Torr

3: mCPBA / CH₂Cl₂

4: AcOH / CH₂Cl₂ / 24 h

With quinoline; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; Pd-BaSO₄; In methanol; diethyl ether; dichloromethane; 1: Grignard reaction / 2: Reduction / 3: Epoxidation / 4: Cyclization;