Technology Process of C53H73N13O14S2
There total 8 articles about C53H73N13O14S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide;
In
N,N-dimethyl-formamide;
Ambient temperature;
DOI:10.1021/jm00185a025
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxybenzotriazole monohydrate / dimethylformamide
2: 100 percent / H2 / Pd/C / aq. ethanol / 5 h
3: 51 percent / 1-hydroxybenzotriazole monohydrate, dicyclohexylcarbodiimide / dimethylformamide / Ambient temperature
With
hydrogen; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00185a025
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 95 percent / aq. NaOH, pyridine / 0.5 h
2: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C
3: NH3 / tetrahydrofuran / 0.5 h / -15 °C
4: H2 / 10percent Pd/C / aq. ethanol / 3 h
5: 1-hydroxybenzotriazole monohydrate / dimethylformamide
6: 100 percent / H2 / Pd/C / aq. ethanol / 5 h
7: 51 percent / 1-hydroxybenzotriazole monohydrate, dicyclohexylcarbodiimide / dimethylformamide / Ambient temperature
With
4-methyl-morpholine; pyridine; sodium hydroxide; ammonia; hydrogen; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00185a025
