Technology Process of C25H39BN2O7
There total 9 articles about C25H39BN2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium periodate; ammonium acetate;
In
water; acetone;
at 23 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: benzene / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
4.2: 20 °C
4.3: 2 h
5.1: 4,6-bis(diphenylphosphanyl)phenoxathiine / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 7 h / 80 °C
6.1: sodium periodate; ammonium acetate / water; acetone / 12 h / 23 °C
With
titanium(IV) isopropylate; sodium periodate; 4,6-bis(diphenylphosphanyl)phenoxathiine; ammonium acetate; trimethylaluminum; pyridine hydrogenfluoride;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; pyridine; hexane; dichloromethane; water; acetone; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 2 h
2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
3.2: 20 °C
3.3: 2 h
4.1: 4,6-bis(diphenylphosphanyl)phenoxathiine / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 7 h / 80 °C
5.1: sodium periodate; ammonium acetate / water; acetone / 12 h / 23 °C
With
titanium(IV) isopropylate; sodium periodate; 4,6-bis(diphenylphosphanyl)phenoxathiine; ammonium acetate; trimethylaluminum; pyridine hydrogenfluoride;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; pyridine; hexane; dichloromethane; water; acetone; toluene;