5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

Base Information

Chemical Name:5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester
CAS No.:129199-22-0
Molecular Formula:C₂₇H₁₉NO₆
Molecular Weight:453.451
Hs Code.:

Synonyms:5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

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Chemical Property of 5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

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Technology Process of 5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

There total 4 articles about 5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 129199-21-9
(2R,3S)-3-Benzoylamino-3-phenyl-2-(2-trimethylsilanyl-ethoxymethoxy)-propionic acid 2-oxo-2H-naphtho[1,8-bc]furan-6-yl ester

: 129199-22-0
5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

Guidance literature:: With hydrogen fluoride; In acetonitrile; for 168h; Ambient temperature;

Reference yield:

: 99458-22-7
(2R,3S)-N-benzoyl-O-<<2-(trimethylsilyl)ethoxy>methyl>-3-phenylisoserine

: 129199-22-0
5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / 4-dimethylaminopyridine, 2-dipyridylcarbonate / tetrahydrofuran / 24 h / 20 °C

2: 80 percent / 40percent aq. HF / acetonitrile / 168 h / Ambient temperature

With dmap; 2,2'-dipyridyl carbonate; hydrogen fluoride; In tetrahydrofuran; acetonitrile;

Reference yield:

: 5656-88-2
6-hydroxy-2H-naphtho<1,8-b,c>furan-2-one

: 129199-22-0
5-hydroxy-1,8-naphthalene carbolactone (2R,3S)-N-benzoyl-3-phenylisoserine ester

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / 4-dimethylaminopyridine, 2-dipyridylcarbonate / tetrahydrofuran / 24 h / 20 °C

2: 80 percent / 40percent aq. HF / acetonitrile / 168 h / Ambient temperature

With dmap; 2,2'-dipyridyl carbonate; hydrogen fluoride; In tetrahydrofuran; acetonitrile;