2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

Base Information

Chemical Name:2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide
CAS No.:1424279-87-7
Molecular Formula:C₂₁H₁₆Cl₃F₃N₂O₃S
Molecular Weight:539.79
Hs Code.:

Synonyms:2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

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Chemical Property of 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

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Technology Process of 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

There total 5 articles about 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1424279-91-3
2-methyl-N-(thietan-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

: 1424279-87-7
2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

: 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5R)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 0.166667h;

Reference yield:

: 1424279-89-9
tert-butyl 2-methyl-4-[(Z)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-enoyl]benzoate

: 1424279-87-7
2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

: 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5R)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1-anthracen-9-ylmethyl quininium chloride; hydroxylamine; caesium hydroxide hydrate / water; chloroform / 16.5 h / -30 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

3: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.33 h / 20 - 30 °C / Inert atmosphere

4: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 - 5 °C

With oxalyl dichloride; caesium hydroxide hydrate; hydroxylamine; triethylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; 1-anthracen-9-ylmethyl quininium chloride; In dichloromethane; chloroform; water;

Reference yield:

: 1424279-90-2
2-methyl-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzoic acid

: 1424279-87-7
2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5S)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

: 2-methyl-N-(1-oxidothietan-1-ium-3-yl)-4-[(5R)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazol-3-yl]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.33 h / 20 - 30 °C / Inert atmosphere

2: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / 0 - 5 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;