6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

Base Information

Chemical Name:6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]
CAS No.:853019-88-2
Molecular Formula:C₂₄H₂₉N₃O₂
Molecular Weight:391.513
Hs Code.:

Synonyms:6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

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Technology Process of 6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

There total 5 articles about 6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853020-65-2
6-methoxy-9-methyl-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

: 589-10-6
phenoxyethyl bromide

: 853019-88-2
6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃;

Reference yield:

: 853020-88-9,853020-89-0,853020-91-4
1'-benzyl-6-methoxy-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

: 853019-88-2
6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / diethyl ether

2.1: dmap / tert-butyl alcohol / 20 - 60 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 2.17 h / 0 - 20 °C

3.2: 1 h / 20 °C

4.1: potassium carbonate / acetonitrile / 70 °C

With hydrogenchloride; sodium hydride; potassium carbonate; dmap; In diethyl ether; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1'-benzyl-6-methoxy-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine] dihydrochloride

: 853019-88-2
6-methoxy-9-methyl-1'-(2-phenoxyethyl)-2,3,4,9-tetrahydrospiro[β-carboline-1,3'-pyrrolidine]

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / tert-butyl alcohol / 20 - 60 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 2.17 h / 0 - 20 °C

2.2: 1 h / 20 °C

3.1: potassium carbonate / acetonitrile / 70 °C

With sodium hydride; potassium carbonate; dmap; In N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;