C₃₂H₅₀N₂O₇S

Base Information

Chemical Name:C₃₂H₅₀N₂O₇S
CAS No.:1362120-15-7
Molecular Formula:C₃₂H₅₀N₂O₇S
Molecular Weight:606.824
Hs Code.:

C<sub>32</sub>H<sub>50</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₃₂H₅₀N₂O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₅₀N₂O₇S

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Technology Process of C₃₂H₅₀N₂O₇S

There total 29 articles about C₃₂H₅₀N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1362120-03-3
C₃₂H₅₂N₂O₇S

: 1362120-15-7
C₃₂H₅₀N₂O₇S

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2.25h;
DOI:10.1021/ol300342n

Reference yield:

: C₁₃H₂₃NO₃

: 1362120-15-7
C₃₂H₅₀N₂O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2.5 h

2.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 3 h / -20 °C

2.2: 3.5 h / -20 - 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

3.2: 2 h / -78 °C

4.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C

5.1: tributylphosphine / tetrahydrofuran / 12.5 h / 0 - 20 °C

6.1: ammonium molybdate; dihydrogen peroxide / ethanol; water / 12 h

7.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.02 h / -78 °C

7.2: 0.33 h / -78 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.25 h / 0 - 20 °C

With methanol; sodium chlorite; lithium borohydride; ammonium molybdate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; tributylphosphine; dihydrogen peroxide; sodium hexamethyldisilazane; pivaloyl chloride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; tert-butyl alcohol; 1.1: Pinnick oxidation;
DOI:10.1021/ol300342n

Reference yield:

: C₁₃H₂₃NO₄

: 1362120-15-7
C₃₂H₅₀N₂O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 3 h / -20 °C

1.2: 3.5 h / -20 - 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 2 h / -78 °C

3.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C

4.1: tributylphosphine / tetrahydrofuran / 12.5 h / 0 - 20 °C

5.1: ammonium molybdate; dihydrogen peroxide / ethanol; water / 12 h

6.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.02 h / -78 °C

6.2: 0.33 h / -78 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.25 h / 0 - 20 °C

With methanol; lithium borohydride; ammonium molybdate; tributylphosphine; dihydrogen peroxide; sodium hexamethyldisilazane; pivaloyl chloride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1021/ol300342n