N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

Base Information

Chemical Name:N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide
CAS No.:1384275-70-0
Molecular Formula:C₂₃H₂₇F₃N₄O₃
Molecular Weight:464.488
Hs Code.:

Synonyms:N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

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Chemical Property of N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

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Technology Process of N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

There total 7 articles about N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1384276-75-8
C₁₅H₂₂N₄O₃

: 402-49-3
4-bromomethyltrifluoromethylbenzene

: 1384275-70-0
N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 12h; Inert atmosphere;

Reference yield:

: 1384276-64-5
2-((5-acetylpyridin-2-yl)amino)acetic acid

: 1384275-70-0
N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethylmorpholine; / N,N-dimethyl-formamide / 2 h / 25 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 1 h / Reflux

3: caesium carbonate / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

With N-ethylmorpholine;; hydroxylamine hydrochloride; sodium acetate; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1384276-76-9
C₁₅H₂₁N₃O₃

: 1384275-70-0
N-((tetrahydro-2H-pyran-4-yl)methyl)-2-((5-(1-(((4-(trifluoromethyl) benzyl)oxy)imino)ethyl)pyridin-2-yl)amino)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 1 h / Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium acetate; caesium carbonate; In ethanol; water; N,N-dimethyl-formamide;