1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

Base Information

Chemical Name:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine
CAS No.:125057-12-7
Molecular Formula:C₂₀H₃₀N₂O₅SSi
Molecular Weight:438.62
Hs Code.:

Synonyms:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

Suppliers and Price of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

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Chemical Property of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

Chemical Property:

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Technology Process of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

There total 1 articles about 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 123027-51-0
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylthio)thymine

: 125057-12-7
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; Ambient temperature;
DOI:10.1021/jm00105a055

Reference yield: 48.0%

: 72886-42-1
methyl 3-sulfanylbenzoate

: 125057-12-7
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

: 137915-51-6
1-<<2-(tert-butyldimethylsiloxy)ethoxy>methyl>-6-<<3-(methoxycarbonyl)phenyl>thio>thymine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 1.5h; Ambient temperature;
DOI:10.1021/jm00080a020

Reference yield:

: 125057-12-7
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylsulfinyl)thymine

: 3-{3-[2-(tert-Butyl-dimethyl-silanyloxy)-ethoxymethyl]-5-methyl-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidin-4-ylsulfanyl}-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature

2: 88 percent / aq. NaOH / tetrahydrofuran; ethanol / 1 h / Ambient temperature

3: N-hydroxysuccinimide, DCC / dioxane / 1 h / Ambient temperature

With sodium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00080a020