1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

Base Information

Chemical Name:1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene
CAS No.:957774-14-0
Molecular Formula:C₂₅H₂₇BrO₃
Molecular Weight:455.392
Hs Code.:

Synonyms:1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

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Chemical Property of 1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

Chemical Property:

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Technology Process of 1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

There total 10 articles about 1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957774-13-9
[4-(benzyloxy)-5-bromo-2-methylphenyl][4-[2-(methoxymethoxy)ethyl]phenyl]methanol

: 957774-14-0
1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 0.25h;

Reference yield:

: 608119-82-0
1-(4-(benzyloxy)-2-methylphenyl)ethanone

: 957774-14-0
1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

Guidance literature:: Multi-step reaction with 7 steps

1.1: Oxone; sodium bromide / water / 2.5 h / 20 °C

2.1: potassium hydroxide; sodium hypochlorite / water / 1 h / 120 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 1 h / 120 °C

4.1: triethylamine / chloroform / 1 h / 0 - 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -10 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

6.2: 1.5 h / -78 °C

7.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 0 °C

With triethylsilane; Oxone; potassium hydroxide; sodium hypochlorite; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; boron trifluoride diethyl etherate; triethylamine; sodium bromide; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; chloroform; water; acetonitrile;

Reference yield:

: 957774-01-5
4-benzyloxy-5-bromo-2-methylbenzoic acid

: 957774-14-0
1-benzyloxy-2-bromo-5-methyl-4-[4-[2-(methoxymethoxy)ethyl]benzyl]benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 1 h / 120 °C

2.1: triethylamine / chloroform / 1 h / 0 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -10 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

4.2: 1.5 h / -78 °C

5.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 0 °C

With triethylsilane; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; boron trifluoride diethyl etherate; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; hexane; chloroform; acetonitrile;