3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

Base Information

Chemical Name:3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol
CAS No.:163580-29-8
Molecular Formula:C₂₈H₂₈O₄
Molecular Weight:428.528
Hs Code.:

Synonyms:3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

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Chemical Property of 3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

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Technology Process of 3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

There total 7 articles about 3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 853260-31-8
((2R,3R,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-ylethynyl)-trimethyl-silane

: 163580-29-8
3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

Guidance literature:: With potassium carbonate; In methanol;
DOI:10.1016/j.tetlet.2005.03.017

Reference yield: 38.0%

: 4,5,7-tri-O-benzyl-1,2-dideoxy-2-O-(4-tolylsulfonyl)-3-O-(triisopropysilyl)-L-ido-hept-1-ynitol

: 3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-gluco-heptitol

: 163580-29-8
3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

: (4S,5S,6R,7R)-5,6-bis(benzyloxy)-7-[(benzyloxy)methyl]-4,5,6,7-tetrahydro-4-[(triisopropylsilyl)oxy][1,2,3]triazolo[1,5-a]pyridine

: (4R,5S,6R,7R)-5,6-bis(benzyloxy)-7-[(benzyloxy)methyl]-4,5,6,7-tetrahydro-4-[(triisopropylsilyl)oxy][1,2,3]triazolo[1,5-a]pyridine

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 110 ℃; for 15h;
DOI:10.1002/(SICI)1522-2675(20000315)83:3<513::AID-HLCA513>3.0.CO;2-1

Reference yield:

: 163396-29-0
(3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2-ethynyl-tetrahydro-furan-2-ol

: 3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-gluco-heptitol

: 163580-29-8
3,6-anhydro-4,5,7-tri-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-D-manno-heptitol

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) -78 deg C, 1 h, 2.) -10 deg C, 12 h;