Technology Process of C42H58O8Si
There total 17 articles about C42H58O8Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium p-toluenesulfonate;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/ol301795a
- Guidance literature:
-
With
pyridinium p-toluenesulfonate; gold(I) chloride;
In
tetrahydrofuran;
at 20 ℃;
for 0.666667h;
Inert atmosphere;
DOI:10.1021/ol301795a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: magnesium bromide diethyl etherate / dichloromethane / -78 - 0 °C / Inert atmosphere
2: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 35 °C / Inert atmosphere
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3.5 h / 0 - 20 °C / pH 7 / aq. buffer; Inert atmosphere
4: pyridinium p-toluenesulfonate; gold(I) chloride / tetrahydrofuran / 0.67 h / 20 °C / Inert atmosphere
With
magnesium bromide diethyl etherate; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; gold(I) chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol301795a