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C14H15NO4S2

Base Information
  • Chemical Name:C14H15NO4S2
  • CAS No.:1198079-02-5
  • Molecular Formula:C14H15NO4S2
  • Molecular Weight:325.409
  • Hs Code.:
C<sub>14</sub>H<sub>15</sub>NO<sub>4</sub>S<sub>2</sub>

Synonyms:C14H15NO4S2

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Chemical Property of C14H15NO4S2
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Technology Process of C14H15NO4S2

There total 2 articles about C14H15NO4S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
malonic acid; 3-(4,5-Dihydro-thiazol-2-ylsulfanylmethyl)-4-hydroxy-5-methoxy-benzaldehyde; With aniline; In pyridine; for 24h; Closed flask;
at 55 ℃; for 4h;
With hydrogenchloride; In pyridine; water; at 0 ℃; pH=< 2;
Guidance literature:
Multi-step reaction with 3 steps
1.1: acetic anhydride / 24 h / Reflux
1.2: 20 - 40 °C
2.1: triethylamine / N,N-dimethyl-formamide / 60 h / 20 °C
3.1: aniline / pyridine / 24 h / Closed flask
3.2: 4 h / 55 °C
3.3: 0 °C / pH < 2
With acetic anhydride; triethylamine; aniline; In pyridine; N,N-dimethyl-formamide;
Guidance literature:
C14H15NO4S2; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetonitrile; at 0 ℃; for 0.166667h;
1-(3,4,5-trimethoxyphenyl)ethylamine; With triethylamine; In acetonitrile; at 0 - 20 ℃;
upstream raw materials:

malonic acid

3-((dimethylamino)methyl)-4-hydroxy-5-methoxybenzaldehyde

Downstream raw materials:

C24H28N2O6S2

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