p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid

Base Information

• Chemical Name: p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid
• CAS No.: 114656-11-0
• Molecular Formula: C₂₃H₂₇NO₁₁
• Molecular Weight: 493.467

Synonyms:p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid

Chemical Property of p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid

There total 4 articles about p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

tert-butyl p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamate (114643-34-4) → p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid (114656-11-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 3h; Ambient temperature;

DOI:10.1016/0008-6215(87)80249-5

Reference yield:

4-hydroxy-trans-cinnamic acid tert-butyl ester (114643-30-0) → p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid (114656-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / NaOEt / dimethylformamide / 20 h / Ambient temperature

2: 88 percent / 90percent CF₃CO₂H / CH₂Cl₂ / 3 h / Ambient temperature

With sodium ethanolate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(87)80249-5

Reference yield:

Sodium; 4-((E)-2-tert-butoxycarbonyl-vinyl)-phenolate (114627-06-4) → p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid (114656-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / dimethylformamide

2: 88 percent / 90percent CF₃CO₂H / CH₂Cl₂ / 3 h / Ambient temperature

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(87)80249-5

upstream raw materials:

tert-butyl p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamate

4-hydroxy-trans-cinnamic acid tert-butyl ester

Sodium; 4-((E)-2-tert-butoxycarbonyl-vinyl)-phenolate

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

Downstream raw materials:

N¹-p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-galactopyranosyloxy)cinnamoyl-N²,N³-di-tert-butoxycarbonylspermidine

N¹-cinnamoylspermidine dihydrochloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 114656-11-0 p-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)cinnamic acid

Send

Send

Metric Ton KG G Pound L ML

Send

Send